methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate

Base Information

• Chemical Name: methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate
• CAS No.: 1045792-83-3
• Molecular Formula: C₂₃H₃₁N₃O₆
• Molecular Weight: 445.516

Synonyms:methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate

Chemical Property of methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate

Chemical Property:

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Technology Process of methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate

There total 1 articles about methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(3-tert-butoxycarbonylaminophenyl)isoxazole-3-carboxylic acid + methyl 7-aminoheptanoate hydrochloride (17994-94-4) → methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate (1045792-83-3)

Guidance literature:

5-(3-tert-butoxycarbonylaminophenyl)isoxazole-3-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

methyl 7-aminoheptanoate hydrochloride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1021/jm8002894

Reference yield: 30.0%

methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate (1045792-83-3) → C22H30N4O6 (1045792-58-2)

Guidance literature:

With potassium hydroxide; hydroxylamine hydrochloride; In methanol; at 20 ℃; for 0.5h;

DOI:10.1021/jm8002894

Reference yield:

methyl 7-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]heptanoate (1045792-83-3) → C18H23N3O4

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm8002894

upstream raw materials:

methyl 7-aminoheptanoate hydrochloride

Downstream raw materials:

C₂₂H₃₀N₄O₆

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