methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside
CAS No.:1404060-71-4
Molecular Formula:C₃₃H₄₂O₁₃
Molecular Weight:646.689
Hs Code.:

Synonyms:methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

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Technology Process of methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

There total 5 articles about methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1404060-70-3
p-tolyl 2,3-anhydro-4,6-di-O-acetyl-1-thio-β-D-mannopyranoside

: 922733-50-4
methyl 2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

: 1404060-71-4
methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at -40 - -25 ℃;
DOI:10.1016/j.tet.2012.09.037

Reference yield:

: C₃₀H₃₆O₈

: 1404060-71-4
methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Reflux

2: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / -40 - -25 °C

With N-iodo-succinimide; lithium aluminium tetrahydride; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2012.09.037

Reference yield:

: 872593-83-4
p-tolyl 2,3-anhydro-4,6-O-benzylidene-1-thio-β-D-mannopyranoside

: 1404060-71-4
methyl 4-O-(2,3-anhydro-4,6-di-O-acetyl-α-D-mannopyranosyl)-2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / 3 h / 0 °C

2: pyridine

3: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / -40 - -25 °C

With pyridine; N-iodo-succinimide; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/j.tet.2012.09.037