C₄₅H₄₆N₆O₆

Base Information

Chemical Name:C₄₅H₄₆N₆O₆
CAS No.:1357258-86-6
Molecular Formula:C₄₅H₄₆N₆O₆
Molecular Weight:766.897
Hs Code.:

C<sub>45</sub>H<sub>46</sub>N<sub>6</sub>O<sub>6</sub>

Synonyms:C₄₅H₄₆N₆O₆

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Chemical Property of C₄₅H₄₆N₆O₆

Chemical Property:

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Technology Process of C₄₅H₄₆N₆O₆

There total 8 articles about C₄₅H₄₆N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₃₅N₅O₃*(x)ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1357258-86-6
C₄₅H₄₆N₆O₆

Guidance literature:: N-methoxycarbonyl-L-valine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 1h;

C₃₈H₃₅N₅O₃*(x)ClH; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 - 20 ℃; for 15h;

Reference yield:

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 1357258-86-6
C₄₅H₄₆N₆O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium chloride / tetrahydrofuran / 30 - 70 °C

1.2: 20 - 30 °C

2.1: acetic acid / toluene / 8 h / Reflux; Dean Stark apparatus

2.2: 1.17 h / 230 - 245 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 90 °C / Inert atmosphere

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0.17 h / 0 - 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 1 h / 20 °C

5.2: 15 h / 0 - 20 °C

With hydrogenchloride; sodium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; magnesium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 1228551-96-9
(S)-tert-butyl 2-(5-(6-bromonaphthalen-2-yl)-1H-imidazol-2-yl)pyrrolidine-1-carboxylate

: 1357258-86-6
C₄₅H₄₆N₆O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium acetate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 15 h / 85 °C / Inert atmosphere

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 90 °C / Inert atmosphere

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0.17 h / 0 - 20 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 1 h / 20 °C

4.2: 15 h / 0 - 20 °C

With hydrogenchloride; potassium acetate; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; dichloromethane; water; toluene; acetonitrile;