sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Base Information

Chemical Name:sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate
CAS No.:100944-77-2
Molecular Formula:C₁₂H₁₁Cl₂N₂O₅S*Na
Molecular Weight:389.192
Hs Code.:

Synonyms:sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Suppliers and Price of sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

There total 3 articles about sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100945-00-4
5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2(1H)-pyrimidinone

: 100944-77-2
sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Guidance literature:: With sodium hydrogensulfite; In water; RT, 4 h; 100 deg C, 10 min, 5 deg C;

Reference yield:

: 3769-30-0
4-chloro-1-α-chloroethoxybenzene

: 100944-77-2
sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / Et₃N / CH₂Cl₂ / 24 h / Ambient temperature

2: 90 percent / NaHSO₃ / H₂O / RT, 4 h; 100 deg C, 10 min, 5 deg C

With sodium hydrogensulfite; triethylamine; In dichloromethane; water;

Reference yield:

: 115171-64-7
1-Chloro-4-(1-methylsulfanyl-ethoxy)-benzene

: 100944-77-2
sodium 5-chloro-1-<1-(4-chlorophenoxy)ethyl>-2-oxo-1,2,3,4-tetrahydropyrimidine-4-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / SO₂Cl₂

2: 37 percent / Et₃N / CH₂Cl₂ / 24 h / Ambient temperature

3: 90 percent / NaHSO₃ / H₂O / RT, 4 h; 100 deg C, 10 min, 5 deg C

With sulfuryl dichloride; sodium hydrogensulfite; triethylamine; In dichloromethane; water;