C₅₀H₇₂N₂O₁₀SSi

Base Information

• Chemical Name: C₅₀H₇₂N₂O₁₀SSi
• CAS No.: 944941-72-4
• Molecular Formula: C₅₀H₇₂N₂O₁₀SSi
• Molecular Weight: 921.281
• Mol file: 944941-72-4.mol

Synonyms:C₅₀H₇₂N₂O₁₀SSi

Chemical Property of C₅₀H₇₂N₂O₁₀SSi

Chemical Property:

Purity/Quality:

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Technology Process of C₅₀H₇₂N₂O₁₀SSi

There total 1 articles about C₅₀H₇₂N₂O₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C49H68N2O12Si + Hexanethiol (111-31-9) → C50H72N2O10SSi (944941-72-4)

Guidance literature:

With trifluoroacetic acid; In 2,2,2-trifluoroethanol; at 20 ℃;

DOI:10.1002/anie.200700539

Reference yield: 51.0%

C50H72N2O10SSi (944941-72-4) → C38H40N2O9 + C38H40N2O9

Guidance literature:

C₅₀H₇₂N₂O₁₀SSi; With oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 0 ℃;

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 1.5h;

With methanesulfonic acid; In dichloromethane; at 20 ℃; for 1h; Further stages.;

DOI:10.1002/anie.200700539

Reference yield:

C50H72N2O10SSi (944941-72-4) → C50H70N2O10SSi + C50H70N2O10SSi

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 0 ℃; Title compound not separated from byproducts.;

DOI:10.1002/anie.200700539

upstream raw materials:

Hexanethiol

Refernces