N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

Base Information

Chemical Name:N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose
CAS No.:1338054-34-4
Molecular Formula:C₁₆H₂₁NO₄
Molecular Weight:291.347
Hs Code.:

Synonyms:N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

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Chemical Property of N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

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Technology Process of N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

There total 7 articles about N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 112-20-9
n-Nonylamin

: 1338054-28-6
1,2-O-isopropylidene-3,5-di-O-trifluoromethanesulfonyl-α-L-ribofuranose

: 1338054-34-4
N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 16h;
DOI:10.1021/ol2024482

Reference yield:

: 1338054-26-4
1,2;5,6-di-O-isopropylidene-α-L-allofuranose

: 1338054-34-4
N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; water / methanol / 1.5 h / 20 °C

2: sodium periodate / water / 4 h / 20 °C

3: sodium tetrahydroborate / ethanol / 1 h / 20 °C

4: pyridine / dichloromethane / 1.75 h / -30 - -20 °C / Inert atmosphere

5: N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C

With pyridine; sodium tetrahydroborate; sodium periodate; sulfuric acid; water; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ol2024482

Reference yield:

: C₁₂H₁₈O₆

: 1338054-34-4
N-(p-methoxybenzyl)-1,2-O-isopropylidene-3,5-dideoxy-3,5-imino-α-L-xylofuranose

Guidance literature:: Multi-step reaction with 6 steps

1: sodium tetrahydroborate / ethanol; water / 0 - 20 °C

2: sulfuric acid; water / methanol / 1.5 h / 20 °C

3: sodium periodate / water / 4 h / 20 °C

4: sodium tetrahydroborate / ethanol / 1 h / 20 °C

5: pyridine / dichloromethane / 1.75 h / -30 - -20 °C / Inert atmosphere

6: N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C

With pyridine; sodium tetrahydroborate; sodium periodate; sulfuric acid; water; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ol2024482