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Technology Process of (CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

Base Information
  • Chemical Name:(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2
  • CAS No.:1355342-64-1
  • Molecular Formula:C49H50BN5O15
  • Molecular Weight:959.772
  • Hs Code.:
(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OCH<sub>2</sub>CHCH<sub>2</sub>)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)OC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>

Synonyms:(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

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Chemical Property of (CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2
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Technology Process of (CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

There total 11 articles about (CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(CH<sub>2</sub>OC(O)OC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)2C(O)OCH<sub>2</sub>CHCH<sub>2</sub>
1355342-63-0

(CH3)4C2O2BC6H4CH2OC6H2(CH2OC(O)OC6H4NO2)2C(O)OCH2CHCH2

disperse red 1
2872-52-8

disperse red 1

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OCH<sub>2</sub>CHCH<sub>2</sub>)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)OC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>
1355342-64-1

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

Guidance literature:
With DMAP; In dichloromethane; 2 h;
DOI:10.1039/c1ob06667f

Reference yield:

p-hydoroxybenzenesulfonic acid
98-67-9

p-hydoroxybenzenesulfonic acid

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OCH<sub>2</sub>CHCH<sub>2</sub>)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)OC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>
1355342-64-1

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

Guidance literature:
Multi-step reaction with 3 steps
1: methanol
2: Et3N; DMAP / tetrahydrofuran
3: DMAP / dichloromethane
With Et3N; DMAP; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1ob06667f

Reference yield:

C<sub>12</sub>H<sub>14</sub>O<sub>5</sub>
1355342-59-4

C12H14O5

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OCH<sub>2</sub>CHCH<sub>2</sub>)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)OC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>
1355342-64-1

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

Guidance literature:
Multi-step reaction with 5 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
2.2: 12 h / 0 - 20 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / methanol / 0.25 h / 20 °C / Inert atmosphere
4.1: dmap; triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
5.1: dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere
With 1H-imidazole; dmap; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06667f
upstream raw materials:

p-hydoroxybenzenesulfonic acid

(CH3)4C2O2BC6H4CH2OC6H2(CH2OH)2C(O)OCH2CHCH2

4-Nitrophenyl chloroformate

(CH3)4C2O2BC6H4CH2OC6H2(CH2OC(O)OC6H4NO2)2C(O)OCH2CHCH2

Downstream raw materials:

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

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