bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

Base Information

Chemical Name:bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite
CAS No.:268739-35-1
Molecular Formula:C₂₆H₃₈N₃O₁₀P
Molecular Weight:583.576
Hs Code.:

Synonyms:bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

Suppliers and Price of bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

There total 2 articles about bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 921-26-6
N,N-diisopropylphosphoramide dichloride

: 37942-55-5
1-(4,5-Dimethoxy-2-nitrophenyl)-ethanol

: 268739-35-1
bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

Guidance literature:: With triethylamine; In tetrahydrofuran; at -40 - 20 ℃;
DOI:10.1080/00397910008087172

Reference yield:

: 20357-25-9
6-nitroveratraldehyde

: 268739-35-1
bis[1-(4,5-dimethoxy-2-nitrophenyl)ethyl]-N,N-diisopropylphosphoramidite

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / tetrahydrofuran; diethyl ether / 0.25 h / -70 °C

2: 78 percent / Et₃N / tetrahydrofuran / -40 - 20 °C

With triethylamine; In tetrahydrofuran; diethyl ether; 1: Addition / 2: Condensation;
DOI:10.1080/00397910008087172