(E)-4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane

Base Information

• Chemical Name: (E)-4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane
• CAS No.: 150785-46-9
• Molecular Formula: C₃₁H₄₈N₄O₇
• Molecular Weight: 588.745

Synonyms:(E)-4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane

Chemical Property of (E)-4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane

Chemical Property:

Purity/Quality:

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Technology Process of (E)-4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane

There total 6 articles about (E)-4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → (E)-4-2,N3-bis(tert-butoxycarbonyl)-N3-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane (150785-46-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 18.6 g / sat. aq. NaHCO₃ / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 2.) DMF, RT, 3 h

3: 69 percent / tetrahydrofuran; H₂O / 1 h / 50 °C

4: Et₃N / tetrahydrofuran; CH₂Cl₂ / 2 h / Ambient temperature

With sodium hydride; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; dichloromethane; water;

DOI:10.1021/jm00072a016

Reference yield:

3,4-dimethoxy-trans-cinnamic acid (14737-89-4) → (E)-4-2,N3-bis(tert-butoxycarbonyl)-N3-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane (150785-46-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 2 h / Ambient temperature

2: Et₃N / tetrahydrofuran; CH₂Cl₂ / 2 h / Ambient temperature

With triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jm00072a016

Reference yield:

N,N'-bis-Boc-S-methyl-isothiourea (322474-21-5) → (E)-4-2,N3-bis(tert-butoxycarbonyl)-N3-(γ,γ-dimethylallyl)guanidino>-1-<(3,4-dimethoxycinnamoyl)amino>butane (150785-46-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 2.) DMF, RT, 3 h

2: 69 percent / tetrahydrofuran; H₂O / 1 h / 50 °C

3: Et₃N / tetrahydrofuran; CH₂Cl₂ / 2 h / Ambient temperature

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; water;

DOI:10.1021/jm00072a016

upstream raw materials:

C₁₅H₂₁O₇P

4-2,N³-bis(tert-butoxycarbonyl)-N³-(γ,γ-dimethylallyl)guanidino>-1-aminobutane

di-tert-butyl dicarbonate

3,4-dimethoxy-trans-cinnamic acid

Downstream raw materials:

(E)-Caracasanamide

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