C₄₂H₅₈O₉

Base Information

Chemical Name:C₄₂H₅₈O₉
CAS No.:1448230-74-7
Molecular Formula:C₄₂H₅₈O₉
Molecular Weight:706.917
Hs Code.:

C<sub>42</sub>H<sub>58</sub>O<sub>9</sub>

Synonyms:C₄₂H₅₈O₉

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Chemical Property of C₄₂H₅₈O₉

Chemical Property:

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Technology Process of C₄₂H₅₈O₉

There total 12 articles about C₄₂H₅₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₅₆O₉

: 1448230-74-7
C₄₂H₅₈O₉

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 2.25h;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-65-6
C₃₂H₆₇IO₄Si₂

: 1448230-74-7
C₄₂H₅₈O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

1.2: 0.33 h / 20 °C

1.3: 13 h / 50 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

4.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

5.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

6.2: 12 h / 0 - 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

With tetrabutyl ammonium fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; acetic acid; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; pentane;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-61-2
C₂₂H₃₆O₆

: 1448230-74-7
C₄₂H₅₈O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

3.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

4.1: sodium iodide / acetone / 18 h / 50 °C

5.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

5.2: 0.33 h / 20 °C

5.3: 13 h / 50 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

8.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

9.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

10.2: 12 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

With 2,6-dimethylpyridine; dmap; tetrabutyl ammonium fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; acetic acid; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; mineral oil; pentane;
DOI:10.1021/ol4017518