(R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one

Base Information

• Chemical Name: (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one
• CAS No.: 219553-16-9
• Molecular Formula: C₁₈H₂₅ClN₂O₅S
• Molecular Weight: 416.926

Synonyms:(R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one

Chemical Property of (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one

Chemical Property:

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Technology Process of (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one

There total 9 articles about (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethylthio)methyl]piperazin-2-one (219553-15-8) → (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one (219553-16-9)

Guidance literature:

With magnesium monoperoxyphthalate; In methanol; at 0 - 20 ℃;

Reference yield:

Na2S203 + (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethylthio)methyl]piperazin-2-one (219553-15-8) → (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one (219553-16-9)

Guidance literature:

With Monoperoxyphthalic acid, magnesium salt; In methanol;

Reference yield:

(R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethylthio)methyl]piperazin-2-one (219553-15-8) + Na2 S2 O3 → (R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethanesulfonyl)methyl]piperazin-2-one (219553-16-9)

Guidance literature:

With Monoperoxyphthalic acid, magnesium salt; In methanol;

upstream raw materials:

{(R)-2-[(2-Chloro-acetyl)-(3-chloro-phenyl)-amino]-1-ethanesulfonylmethyl-ethyl}-carbamic acid tert-butyl ester

3-chloro-aniline

{1-[(3-chloro-phenylamino)-methyl]-2-ethanesulfonyl-ethyl}-carbamic acid tert-butyl ester

(R)-4-(tert-butoxycarbonyl)-1-(3-chlorophenyl)-5-[(ethylthio)methyl]piperazin-2-one

Downstream raw materials:

(R)-1-(3-chlorophenyl)-4-[1-(4-cyanobenzyl)-5-imidazolylmethyl]-5-[2-(ethanesulfonyl)methyl]-2-piperazinone

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