C₅₀H₅₈NO₁₉P

Base Information

Chemical Name:C₅₀H₅₈NO₁₉P
CAS No.:1428873-05-5
Molecular Formula:C₅₀H₅₈NO₁₉P
Molecular Weight:1007.98
Hs Code.:

C<sub>50</sub>H<sub>58</sub>NO<sub>19</sub>P

Synonyms:C₅₀H₅₈NO₁₉P

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Chemical Property of C₅₀H₅₈NO₁₉P

Chemical Property:

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Technology Process of C₅₀H₅₈NO₁₉P

There total 6 articles about C₅₀H₅₈NO₁₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428872-89-2
C₅₃H₆₂NO₁₉P

: 1428873-05-5
C₅₀H₅₈NO₁₉P

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In acetonitrile; at 0 ℃; for 2h;
DOI:10.1016/j.bmcl.2013.02.068

Reference yield:

: 93451-41-3
allyl-2,3,4-tri-O-benzyl-6-O-trityl-α-D-mannopyranoside

: 1428873-05-5
C₅₀H₅₈NO₁₉P

Guidance literature:: Multi-step reaction with 6 steps

1: ruthenium trichloride; sodium periodate / dichloromethane; acetonitrile; water / 2 h / 20 °C

2: potassium carbonate / dichloromethane / 6 h / 20 °C

3: iron(III) chloride hexahydrate / dichloromethane / 2 h / 0 - 20 °C

4: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 20 °C / Inert atmosphere; Molecular sieve

5: tert.-butylhydroperoxide / water / 2 h / -40 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / acetonitrile / 2 h / 0 °C

With morpholine; 1H-tetrazole; tert.-butylhydroperoxide; ruthenium trichloride; sodium periodate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iron(III) chloride hexahydrate; potassium carbonate; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.068

Reference yield:

: 1428872-86-9
C₅₁H₅₀O₈

: 1428873-05-5
C₅₀H₅₈NO₁₉P

Guidance literature:: Multi-step reaction with 4 steps

1: iron(III) chloride hexahydrate / dichloromethane / 2 h / 0 - 20 °C

2: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 20 °C / Inert atmosphere; Molecular sieve

3: tert.-butylhydroperoxide / water / 2 h / -40 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / acetonitrile / 2 h / 0 °C

With morpholine; 1H-tetrazole; tert.-butylhydroperoxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iron(III) chloride hexahydrate; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.068