Technology Process of C17H17N3
There total 3 articles about C17H17N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
at 20 ℃;
for 6h;
under 2585.74 Torr;
DOI:10.1515/HC.2004.10.6.423
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-BuLi; tetramethylethylenediamine / hexane / 1 h / Heating
1.2: (n-Bu)3SnCl / hexane / 2 h / Heating
1.3: (PPh3)4Pd / dioxane / 90 - 100 °C
2.1: aq. SnCl2 / ethyl acetate / Heating
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tin(ll) chloride;
In
hexane; ethyl acetate;
1.3: Stille coupling;
DOI:10.1016/j.bmcl.2005.05.080
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-BuLi; tetramethylethylenediamine / hexane / 1 h / Heating
1.2: (n-Bu)3SnCl / hexane / 2 h / Heating
1.3: (PPh3)4Pd / dioxane / 90 - 100 °C
2.1: aq. SnCl2 / ethyl acetate / Heating
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tin(ll) chloride;
In
hexane; ethyl acetate;
1.3: Stille coupling;
DOI:10.1016/j.bmcl.2005.05.080