5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole

Base Information

Chemical Name:5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole
CAS No.:1240736-72-4
Molecular Formula:C₂₇H₂₉N₃O₃
Molecular Weight:443.546
Hs Code.:

Synonyms:5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole

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Technology Process of 5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole

There total 1 articles about 5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 4-(2-piperidin-1-ylethoxy)benzyl bromide hydrobromide

: 54998-29-7
ethyl 4-methoxybenzimidate hydrochloride

: 102-51-2
4-methoxy-1,2-phenylenediamine

: 1240736-72-4
5-hydroxy-2-(4-hydroxyphenyl)-1-[4-(2-piperidin-1-ylethoxy)benzyl]-1H-benzimidazole

Guidance literature:: ethyl 4-methoxybenzimidate hydrochloride; 4-methoxy-1,2-phenylenediamine; With aluminum (III) chloride; ethanethiol; In ethanol; at 20 ℃; for 4h; Inert atmosphere; Reflux;

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

4-(2-piperidin-1-ylethoxy)benzyl bromide hydrobromide; Further stages;
DOI:10.1016/j.bmc.2010.06.016