methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Base Information

Chemical Name:methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate
CAS No.:194855-43-1
Molecular Formula:C₂₅H₂₉ClO₄S
Molecular Weight:461.022
Hs Code.:

Synonyms:methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

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Chemical Property of methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

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Technology Process of methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

There total 11 articles about methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150-19-6
O-methylresorcine

: 194855-43-1
methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Guidance literature:: Multi-step reaction with 7 steps

1: Cs₂CO₃ / dimethylformamide

2: CH₃SO₂OH / CH₂Cl₂ / -10 - 20 °C

3: BBr₃ / CH₂Cl₂ / 1 h / -10 - 20 °C

4: Cs₂CO₃ / dimethylformamide

5: 1,2-dichloro-benzene / Heating

6: H₂ / 5 percent Pd/C / various solvent(s) / 0.5 h / 760 Torr

7: Cs₂CO₃ / dimethylformamide

With methanesulfonic acid; hydrogen; boron tribromide; caesium carbonate; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; 5: Claisen rearrangement;
DOI:10.1016/S0960-894X(03)00115-X

Reference yield:

: 29040-42-4
3-ethyl-6-methoxy-benzofuran

: 194855-43-1
methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Guidance literature:: Multi-step reaction with 5 steps

1: BBr₃ / CH₂Cl₂ / 1 h / -10 - 20 °C

2: Cs₂CO₃ / dimethylformamide

3: 1,2-dichloro-benzene / Heating

4: H₂ / 5 percent Pd/C / various solvent(s) / 0.5 h / 760 Torr

5: Cs₂CO₃ / dimethylformamide

With hydrogen; boron tribromide; caesium carbonate; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; 3: Claisen rearrangement;
DOI:10.1016/S0960-894X(03)00115-X

Reference yield:

: 3-ethyl-benzofuran-6-ol

: 194855-43-1
methyl 3-chloro-4-(3-(3-ethyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: Cs₂CO₃ / dimethylformamide

2: 1,2-dichloro-benzene / Heating

3: H₂ / 5 percent Pd/C / various solvent(s) / 0.5 h / 760 Torr

4: Cs₂CO₃ / dimethylformamide

With hydrogen; caesium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; 2: Claisen rearrangement;
DOI:10.1016/S0960-894X(03)00115-X