C₃₆H₄₄O₁₄

Base Information

Chemical Name:C₃₆H₄₄O₁₄
CAS No.:1286209-82-2
Molecular Formula:C₃₆H₄₄O₁₄
Molecular Weight:700.737
Hs Code.:

C<sub>36</sub>H<sub>44</sub>O<sub>14</sub>

Synonyms:C₃₆H₄₄O₁₄

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Chemical Property of C₃₆H₄₄O₁₄

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Technology Process of C₃₆H₄₄O₁₄

There total 1 articles about C₃₆H₄₄O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1204206-79-0
C₄₃H₅₀O₁₄

: 1286209-82-2
C₃₆H₄₄O₁₄

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In ethyl acetate; at 20 ℃; for 24h; under 750.075 Torr;
DOI:10.1002/chem.201003399

Reference yield:

: 1286209-82-2
C₃₆H₄₄O₁₄

: C₃₆H₄₂O₁₄

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - -10 ℃; for 1.5h;
DOI:10.1002/chem.201003399

Reference yield:

: 1286209-82-2
C₃₆H₄₄O₁₄

: C₅₁H₇₈O₁₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1.5 h / -78 - -10 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -13 - 0 °C

2.2: -78 °C

2.3: -78 - -10 °C

3.1: dmap / dichloromethane / 16.5 h / 0 - 20 °C

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 3 h / Reflux

5.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 0 - 20 °C

6.1: methanol; potassium carbonate / 2.5 h / 16 °C

7.1: 4-pyrrolidin-1-ylpyridine; triethylamine / dichloromethane / 17.5 h / -3 °C

8.1: dmap / dichloromethane / 3 h / 0 - 20 °C

9.1: diethylzinc / toluene / 0 °C

9.2: 0.5 h / 0 °C

9.3: 19.5 h / 0 - 20 °C

10.1: Ru(OCOCH₃)2{(S)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl)}; hydrogen / methanol / 10 h / 20 °C / 41254.1 Torr

11.1: dmap / dichloromethane / 3.5 h / 0 °C

With methanol; dmap; n-butyllithium; oxalyl dichloride; Ru(OCOCH₃)2{(S)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl)}; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; hydrogen; diethylzinc; tri-n-butyl-tin hydride; potassium carbonate; 4-pyrrolidin-1-ylpyridine; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; benzene; 1.1: Swern oxidation;
DOI:10.1002/chem.201003399