3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

Base Information

Chemical Name:3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol
CAS No.:157547-47-2
Molecular Formula:C₂₀H₂₆O₃
Molecular Weight:314.425
Hs Code.:

Synonyms:3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

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Chemical Property of 3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

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Technology Process of 3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

There total 4 articles about 3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 157547-46-1
6-benzyloxy-4,4,5,7-tetramethylhydrocoumarin

: 157547-47-2
3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 7h;
DOI:10.1248/cpb.48.238

Reference yield:

: 50442-68-7
6-hydroxy-4,4,5,7-tetramethyl-3,4-dihydrocoumarin

: 157547-47-2
3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃; NaI / acetone / 20 h / Heating

2: 97 percent / LiAlH₄ / tetrahydrofuran / 7 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; sodium iodide; In tetrahydrofuran; acetone; 1: Alkylation / 2: Reduction;
DOI:10.1248/cpb.48.238

Reference yield:

: 100-44-7
benzyl chloride

: 157547-47-2
3-(2'-Hydroxy-5'-benzyloxy-4',6'-dimethylphenyl)-3,3-dimethyl-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃; NaI / acetone / 20 h / Heating

2: 97 percent / LiAlH₄ / tetrahydrofuran / 7 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; sodium iodide; In tetrahydrofuran; acetone; 1: Alkylation / 2: Reduction;
DOI:10.1248/cpb.48.238