C₁₉H₂₃NO₂S

Base Information

Chemical Name:C₁₉H₂₃NO₂S
CAS No.:862563-57-3
Molecular Formula:C₁₉H₂₃NO₂S
Molecular Weight:329.463
Hs Code.:

C<sub>19</sub>H<sub>23</sub>NO<sub>2</sub>S

Synonyms:C₁₉H₂₃NO₂S

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Chemical Property of C₁₉H₂₃NO₂S

Chemical Property:

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Technology Process of C₁₉H₂₃NO₂S

There total 13 articles about C₁₉H₂₃NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 862563-61-9
C₂₀H₂₂F₃NO₅S₂

: 862563-57-3
C₁₉H₂₃NO₂S

Guidance literature:: With formic acid; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 60 ℃; for 5h;
DOI:10.1021/ol051184v

Reference yield:

: 172825-16-0
(1R)-1-methyl-2-oxo-cyclohexanecarboxylic acid ethyl ester

: 862563-57-3
C₁₉H₂₃NO₂S

Guidance literature:: Multi-step reaction with 10 steps

1.1: P₂O₅ / CH₂Cl₂ / 48 h / 23 °C

2.1: DIBAL-H / toluene; hexane / 0.33 h / 0 °C

3.1: 0.188 g / IBX / dimethylsulfoxide / 4 h / 23 °C

4.1: 94 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

5.1: Et₃N; molecular sieves 3 Angstroem / methanol / 12 h / 23 °C

6.1: 0.38 g / NaBH₄ / methanol / 0.5 h

7.1: 77 percent / Br₂; AcOH / H₂O; methanol / 2.5 h / 0 °C

8.1: 70 percent / toluene / 15 h / 120 °C

9.1: L-Selectride / tetrahydrofuran / 1 h / -78 °C

9.2: 72 percent / tetrahydrofuran / -78 - 23 °C

10.1: 84 percent / Et₃N; formic acid / PdCl₂(PPh₃)2 / dimethylformamide / 5 h / 60 °C

With sodium tetrahydroborate; formic acid; 3 A molecular sieve; bromine; phosphorus pentoxide; L-Selectride; diisobutylaluminium hydride; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol051184v

Reference yield:

: 862563-52-8
1-methyl-2-phenylsulfanyl-cyclohex-2-enecarbaldehyde

: 862563-57-3
C₁₉H₂₃NO₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 94 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

2.1: Et₃N; molecular sieves 3 Angstroem / methanol / 12 h / 23 °C

3.1: 0.38 g / NaBH₄ / methanol / 0.5 h

4.1: 77 percent / Br₂; AcOH / H₂O; methanol / 2.5 h / 0 °C

5.1: 70 percent / toluene / 15 h / 120 °C

6.1: L-Selectride / tetrahydrofuran / 1 h / -78 °C

6.2: 72 percent / tetrahydrofuran / -78 - 23 °C

7.1: 84 percent / Et₃N; formic acid / PdCl₂(PPh₃)2 / dimethylformamide / 5 h / 60 °C

With sodium tetrahydroborate; formic acid; 3 A molecular sieve; bromine; L-Selectride; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol051184v