Technology Process of C22H26O6S
There total 2 articles about C22H26O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di(n-butyl)tin oxide; triethylamine;
In
dichloromethane;
at 20 ℃;
for 14h;
DOI:10.1021/ol902217q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 - -50 °C
1.2: -78 - 20 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 13 h / 0 - 20 °C
3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide / dichloromethane / 9 h / -40 - -25 °C / Molecular sieve
3.2: 1.5 h / -25 - 20 °C
4.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 13.83 h / 20 °C
With
titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; di(n-butyl)tin oxide; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane;
3.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2010.11.017
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 4h;
DOI:10.1021/ol902217q