N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

Base Information

Chemical Name:N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine
CAS No.:1089275-53-5
Molecular Formula:C₃₀H₃₆N₆O
Molecular Weight:496.655
Hs Code.:

Synonyms:N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

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Chemical Property of N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

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Technology Process of N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

There total 3 articles about N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 20662-53-7
4-(2-keto-1-benzimidazolinyl)piperidine

: (S)-N,N-dibenzylpropane-1,2-diamine

: 104619-51-4
di(1H-imidazol-1-yl)methanimine

: 1089275-53-5
N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

Guidance literature:: 4-(2-keto-1-benzimidazolinyl)piperidine; di(1H-imidazol-1-yl)methanimine; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 72h;

(S)-N,N-dibenzylpropane-1,2-diamine; In tetrahydrofuran; N,N-dimethyl-formamide; for 72h; Heating / reflux;

Reference yield:

: 1087312-07-9
2-((S)-2-(dibenzylamino)propyl)isoindoline-1,3-dione

: 1089275-53-5
N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine / ethanol / 3 h / 20 °C / Heating / reflux

2.1: tetrahydrofuran; N,N-dimethyl-formamide / 72 h / 20 °C

2.2: 72 h / Heating / reflux

With hydrazine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 60479-65-4
(S)-2-(N,N-dibenzylamino)-1-propanol

: 1089275-53-5
N-((S)-2-(dibenzylamino)propyl)-4-(1,2-dihydro-2-oxobenzo[d]imidazol-3-yl)piperidine-1-carboxamidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C

2.1: hydrazine / ethanol / 3 h / 20 °C / Heating / reflux

3.1: tetrahydrofuran; N,N-dimethyl-formamide / 72 h / 20 °C

3.2: 72 h / Heating / reflux

With triphenylphosphine; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;