(E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Base Information

Chemical Name:(E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline
CAS No.:1334306-19-2
Molecular Formula:C₅₁H₅₉N
Molecular Weight:686.036
Hs Code.:

Synonyms:(E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Suppliers and Price of (E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

There total 4 articles about (E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1334306-18-1
(E)-7-(4-(diphenylamino)styryl)-9,9-dioctyl-9H-fluorene-2-carbaldehyde

: 2065-66-9
methyl-triphenylphosphonium iodide

: 1334306-19-2
(E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Guidance literature:: methyl-triphenylphosphonium iodide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 0.25h;

(E)-7-(4-(diphenylamino)styryl)-9,9-dioctyl-9H-fluorene-2-carbaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.tet.2011.09.008

Reference yield:

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 1334306-19-2
(E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 - 20 °C

1.2: 3 h / 0 - 20 °C

2.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 - 20 °C

3.2: 3 h / 0 - 20 °C

With potassium tert-butylate; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; 1.2: Wittig reaction / 2.1: Heck reaction / 3.2: Wittig reaction;
DOI:10.1016/j.tet.2011.09.008

Reference yield:

: 25069-74-3
N,N-diphenyl-N-(4-vinylphenyl)amine

: 1334306-19-2
(E)-4-(2-(9,9-dioctyl-7-vinyl-9H-fluoren-2-yl)vinyl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 - 20 °C

2.2: 3 h / 0 - 20 °C

With potassium tert-butylate; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Heck reaction / 2.2: Wittig reaction;
DOI:10.1016/j.tet.2011.09.008