Technology Process of (+/-)-faveline methyl ether
There total 1 articles about (+/-)-faveline methyl ether which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 9 steps
1: 95 percent / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
2: 90 percent / carbon tetrachloride; triphenylphosphine / acetonitrile / 7 h / 20 °C
3: 57 percent / lithium / tetrahydrofuran / -10 - 0 °C
4: 86 percent / N-bromosuccinimide / acetonitrile / 4 h / -20 °C
5: 88 percent / zinc; ammonium chloride / diethyl ether / 20 °C
6: 83 percent / potassium carbonate; triphenylphosphine; palladium(II) acetate / acetonitrile / Heating
7: N-methylmorpholine oxide; osmium tetroxide / 2-methyl-propan-2-ol; acetone; H2O / 0 - 20 °C
8: 268 mg / sodium periodate / methanol; H2O / 0 - 20 °C
9: 28 percent / potassium hydrogen sulfate / 0.75 h / 190 °C
With
tetrachloromethane; sodium periodate; potassium hydrogensulfate; N-Bromosuccinimide; osmium(VIII) oxide; lithium aluminium tetrahydride; ammonium chloride; palladium diacetate; lithium; potassium carbonate; 4-methylmorpholine N-oxide; triphenylphosphine; zinc;
In
tetrahydrofuran; methanol; diethyl ether; water; acetone; acetonitrile; tert-butyl alcohol;
3: Barbier reaction / 6: Heck reaction;
DOI:10.1021/jo051082i