6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

Base Information

Chemical Name:6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine
CAS No.:1591908-14-3
Molecular Formula:C₃₀H₁₉N₅O₂S₃
Molecular Weight:577.711
Hs Code.:

Synonyms:6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

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Chemical Property of 6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

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Technology Process of 6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

There total 6 articles about 6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 56278-50-3
2-cyanomethylbenzothiazole

: 1591908-08-5
1-(benzothiazol-2-yl)-2-(2-phenylhydrazono)-2-(phenylsulfonyl)ethanone

: 1591908-14-3
6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

Guidance literature:: With triethylamine; In ethanol; at 150 ℃; for 0.25h; under 12901.3 Torr; Microwave irradiation;
DOI:10.3987/COM-13-12873

Reference yield:

: 54223-20-0
1-(benzo[d]thiazol-2-yl)-2-bromoethanone

: 1591908-14-3
6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 3 h / Reflux

2.1: sodium acetate / ethanol / 0.17 h

2.2: 6.5 h / 0 - 4 °C

3.1: triethylamine / ethanol / 0.25 h / 150 °C / 12901.3 Torr / Microwave irradiation

With sodium acetate; triethylamine; In ethanol;
DOI:10.3987/COM-13-12873

Reference yield:

: 1591907-98-0
1-(benzothiazol-2-yl)-2-phenylsulfonyl-1-ethanone

: 1591908-14-3
6-(benzenesulfonyl)-4,5-bis(1,3-benzothiazol-2-yl)-2-phenyl-2,3-dihydropyridazin-3-imine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / ethanol / 0.17 h

1.2: 6.5 h / 0 - 4 °C

2.1: triethylamine / ethanol / 0.25 h / 150 °C / 12901.3 Torr / Microwave irradiation

With sodium acetate; triethylamine; In ethanol;
DOI:10.3987/COM-13-12873