rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

Base Information

Chemical Name:rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester
CAS No.:170728-75-3
Molecular Formula:C₂₁H₂₆O₅
Molecular Weight:358.434
Hs Code.:

Synonyms:rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

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Chemical Property of rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

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Technology Process of rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

There total 3 articles about rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6093-67-0
5-hydroxycoumarin

: 170728-75-3
rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; trifluoromethanesulfonic acid anhydride / dichloromethane

2: copper(I) iodide; triethylamine / dichlorobis(triphenylphosphine)palladium[II] / N,N-dimethyl-formamide

3: hydrogenchloride / methanol

With pyridine; hydrogenchloride; copper(I) iodide; trifluoromethanesulfonic acid anhydride; triethylamine; dichlorobis(triphenylphosphine)palladium[II]; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

methanolic sodium methoxide: methanolic sodium methoxide

: rac-5-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-2H-1-benzopyran-2-one

: 170728-75-3
rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

Guidance literature:: With hydrogenchloride; In methanol;

Reference yield:

: 150598-37-1
trifluoromethanesulfonic acid 2-oxo-2H-1-benzopyran-5-yl ester

: 170728-75-3
rac-(E)-3-[2-Hydroxy-6-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]-phenyl]-2-propenoic Acid Methyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: copper(I) iodide; triethylamine / dichlorobis(triphenylphosphine)palladium[II] / N,N-dimethyl-formamide

2: hydrogenchloride / methanol

With hydrogenchloride; copper(I) iodide; triethylamine; dichlorobis(triphenylphosphine)palladium[II]; In methanol; N,N-dimethyl-formamide;