(3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

Base Information

Chemical Name:(3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone
CAS No.:1370016-01-5
Molecular Formula:C₂₉H₂₂O₆S₂
Molecular Weight:530.622
Hs Code.:

Synonyms:(3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

Suppliers and Price of (3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

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Chemical Property of (3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

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Technology Process of (3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

There total 3 articles about (3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 83806-46-6
(5-bromo-1-benzofuran-2-yl)(4-bromophenyl)methanone

: 373384-18-0
3-(methanesulfonyl)phenylboronic acid

: 1370016-01-5
(3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

Guidance literature:: (5-bromo-1-benzofuran-2-yl)(4-bromophenyl)methanone; 3-(methanesulfonyl)phenylboronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 110 ℃; for 5h; Inert atmosphere;

With dihydrogen peroxide; In ethanol; water; toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1007/s00044-012-0017-y

Reference yield:

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 1370016-01-5
(3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; sodium carbonate / water / 5 h / 80 °C

2.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene; ethanol / 5 h / 110 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; 2.1: |Suzuki Coupling;
DOI:10.1007/s00044-012-0017-y

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 1370016-01-5
(3'-methanesulfonylbiphenyl-4-yl)[5-(3-methanesulfonylphenyl)benzofuran-2-yl]methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; sodium carbonate / water / 5 h / 80 °C

2.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene; ethanol / 5 h / 110 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; 2.1: |Suzuki Coupling;
DOI:10.1007/s00044-012-0017-y