1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

Base Information

Chemical Name:1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride
CAS No.:1333493-60-9
Molecular Formula:C₂₄H₃₉NO₃*ClH
Molecular Weight:426.039
Hs Code.:

Synonyms:1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

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Chemical Property of 1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

Chemical Property:

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Technology Process of 1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

There total 4 articles about 1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333493-68-7
1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione

: 1333493-60-9
1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

Guidance literature:: With hydrogenchloride; In water; at 5 ℃;

Reference yield:

: 539-82-2
ethyl n-valerate

: 1257220-36-2
4'-[3-(di-n-butylamino)propoxy]acetophenone

: 1333493-60-9
1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

Guidance literature:: ethyl n-valerate; 4'-[3-(di-n-butylamino)propoxy]acetophenone; With sodium methylate; In 1-methyl-pyrrolidin-2-one; at 5 - 20 ℃;

With hydrogenchloride; In 1-methyl-pyrrolidin-2-one; water; at 5 ℃;

Reference yield:

: 36421-15-5
dibutyl-(3-chloro-propyl)-amine

: 1333493-60-9
1-{4-[3-(di-n-butylamino)propoxy]phenyl}-1,3-heptanedione hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / butanone / Reflux

2.1: sodium methylate / 1-methyl-pyrrolidin-2-one / 5 - 20 °C

2.2: 5 °C

With sodium methylate; potassium carbonate; In 1-methyl-pyrrolidin-2-one; butanone;