2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid

Base Information

Chemical Name:2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid
CAS No.:1206481-50-6
Molecular Formula:C₃₆H₄₄O₁₀
Molecular Weight:636.739
Hs Code.:

Synonyms:2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid

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Chemical Property of 2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid

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Technology Process of 2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid

There total 1 articles about 2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1206481-49-3
2-(trimethylsilyl)ethyl 2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-(tert-butyldimethylsilyloxy)pentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoate

: 1206481-50-6
2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tet.2009.11.024

Reference yield: 77.0%

: 1206481-50-6
2-((E)-3-((2S,4R,5S,6S)-6-((R)-4-hydroxypentyl)-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)prop-1-enyl)-3,4,6-trimethoxybenzoic acid

: 1206481-44-8
C₃₆H₄₂O₉

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.024