4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

Base Information

Chemical Name:4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide
CAS No.:252679-39-3
Molecular Formula:C₂₁H₃₁IO₄
Molecular Weight:474.379
Hs Code.:

Synonyms:4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

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Chemical Property of 4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

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Technology Process of 4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

There total 7 articles about 4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 252679-37-1
4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl alcohol

: 252679-39-3
4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

Guidance literature:: 4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl alcohol; With TEA; methanesulfonyl chloride;

With sodium iodide;
DOI:10.1016/j.tetlet.2004.12.114

Reference yield:

: 252679-38-2
Methanesulfonic acid 4-((E)-3,7-dimethyl-octa-2,6-dienyl)-3,5-bis-methoxymethoxy-benzyl ester

: 252679-39-3
4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 22h;
DOI:10.1021/jo9908795

Reference yield:

: 76280-60-9
[3,5-bis(methoxymethoxy)phenyl]methanol

: 252679-39-3
4-((2E)-3,7-dimethyl-2,6-octadienyl)-3,5-bis(methoxymethoxy)benzyl iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 73 percent / n-BuLi; CuCN / -20 °C

2.1: 86 percent / TBAF

3.1: TEA; MsCl

3.2: 86 percent / NaI

With n-butyllithium; TEA; tetrabutyl ammonium fluoride; methanesulfonyl chloride;
DOI:10.1016/j.tetlet.2004.12.114