1,1'-(2-Chloroethene-1,1-diyl)bis(4-methylbenzene)

Base Information

Chemical Name:1,1'-(2-Chloroethene-1,1-diyl)bis(4-methylbenzene)
CAS No.:5293-66-3
Molecular Formula:C16H15Cl
Molecular Weight:242.748
Hs Code.:
NSC Number:123017
DSSTox Substance ID:DTXSID70967398

Synonyms:5293-66-3;1,1'-(2-chloroethene-1,1-diyl)bis(4-methylbenzene);NSC123017;DTXSID70967398;NSC-123017

Suppliers and Price of 1,1'-(2-Chloroethene-1,1-diyl)bis(4-methylbenzene)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,1'-(2-Chloroethene-1,1-diyl)bis(4-methylbenzene)

Chemical Property:

Boiling Point:345.2°Cat760mmHg
Flash Point:157.3°C
Density:1.082g/cm³
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:242.0862282
Heavy Atom Count:17
Complexity:229

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=CCl)C2=CC=C(C=C2)C

Technology Process of 1,1'-(2-Chloroethene-1,1-diyl)bis(4-methylbenzene)

There total 6 articles about 1,1'-(2-Chloroethene-1,1-diyl)bis(4-methylbenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2919-20-2
1,1-di(p-tolyl)ethylene

: 5293-66-3
4,4'-(2-chloroethene-1,1-diyl)bis(methylbenzene)

Guidance literature:: With N-chloro-succinimide; acetic acid; at 70 ℃; for 4h;
DOI:10.1016/j.tet.2018.11.018

Reference yield:

: 26204-07-9
1,1-dichloro-2,2-bis(p-methylphenyl)ethane

: 5293-66-3
4,4'-(2-chloroethene-1,1-diyl)bis(methylbenzene)

Guidance literature:: With N-isopropyl-N-methylaniline;

Reference yield:

: 611-97-2
bis(p-methylphenyl)-methanone

: 5293-66-3
4,4'-(2-chloroethene-1,1-diyl)bis(methylbenzene)

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere; Cooling

2.1: acetic acid; N-chloro-succinimide / 4 h / 70 °C

With N-chloro-succinimide; n-butyllithium; acetic acid; In tetrahydrofuran; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.1016/j.tet.2018.11.018