N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester

Base Information

Chemical Name:N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester
CAS No.:440321-04-0
Molecular Formula:C₂₉H₃₇NO₄Si
Molecular Weight:491.703
Hs Code.:

Synonyms:N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester

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Chemical Property of N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester

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Technology Process of N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester

There total 2 articles about N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 13515-76-9,116457-91-1,4465-44-5
methyl N-trityl-L-serinate

: 440321-04-0
N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4020(02)00115-1

Reference yield:

: 76-83-5
trityl chloride

: 440321-04-0
N-trityl-(S)-serine 3-[2-(trimethylsilyl)-ethoxymethyl ether] methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NEt₃

2: 97 percent / DIEA / CH₂Cl₂ / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(02)00115-1