2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

Base Information

Chemical Name:2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde
CAS No.:129216-02-0
Molecular Formula:C₁₃H₈Cl₃NO₂
Molecular Weight:316.571
Hs Code.:

Synonyms:2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

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Chemical Property of 2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

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Technology Process of 2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

There total 3 articles about 2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 129215-97-0
2,6-Dichloro-4-(3-chloro-phenyl)-5-[1-dimethylamino-meth-(Z)-ylidene]-4,5-dihydro-pyridine-3-carbaldehyde

: 129216-02-0
2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; Ambient temperature; 0.25-0.5 h;
DOI:10.1021/jo00309a026

Reference yield:

: 113675-65-3
β-(chloro-3 phenyl) glutarimide

: 129216-02-0
2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) POCl₃ / 1.) rt, 3 h 2.) 1,2-dichlorethane, rt, 15 h

2: sodium acetate / H₂O / Ambient temperature; 0.5-2 h

3: 98 percent / 0.5 N hydrochloric acid / tetrahydrofuran / Ambient temperature; 0.25-0.5 h

With hydrogenchloride; sodium acetate; trichlorophosphate; In tetrahydrofuran; water;
DOI:10.1021/jo00309a026

Reference yield:

: C₁₇H₂₀Cl₃N₃⁽²⁺⁾*2Cl^(1-)

: 129216-02-0
2,6-Dichloro-4-(3-chloro-phenyl)-1,4-dihydro-pyridine-3,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / H₂O / Ambient temperature; 0.5-2 h

2: 98 percent / 0.5 N hydrochloric acid / tetrahydrofuran / Ambient temperature; 0.25-0.5 h

With hydrogenchloride; sodium acetate; In tetrahydrofuran; water;
DOI:10.1021/jo00309a026