1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose

Base Information

• Chemical Name: 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose
• CAS No.: 107961-15-9
• Molecular Formula: C₃₁H₃₂O₈
• Molecular Weight: 532.59

Synonyms:1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose

Chemical Property of 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose

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Technology Process of 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose

There total 8 articles about 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

dimethyl diazomalonate (6773-29-1) + β-1-deoxy-1-C-<(phenylthio)bis(methoxycarbonyl)methyl>-2,3,5-tri-O-benzyl-D-ribofuranose (107961-14-8) → 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose (107961-15-9)

Guidance literature:

rhodium(II) acetate; In dichloromethane; for 2.5h; Heating;

DOI:10.1021/ja00244a024

Reference yield: 56.7%

dimethyl diazomalonate (6773-29-1) + α-1-deoxy-1-C-(phenylthio)-2,3,5-tri-O-benzyl-D-ribofuranose (107961-04-6) → 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose (107961-15-9)

Guidance literature:

rhodium(II) acetate; In dichloromethane; for 8h; Heating;

DOI:10.1021/ja00244a024

Reference yield: 4.7%

dimethyl diazomalonate (6773-29-1) + β-1-deoxy-1-C-(phenylthio)-2,3,5-tri-O-benzyl-D-ribofuranose (107961-03-5) → 1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose (107961-15-9) + β-1-deoxy-1-C-<(phenylthio)bis(methoxycarbonyl)methyl>-2,3,5-tri-O-benzyl-D-ribofuranose (107961-14-8)

Guidance literature:

rhodium(II) acetate; In dichloromethane; for 2.5h; Heating;

DOI:10.1021/ja00244a024

upstream raw materials:

dimethyl diazomalonate

β-1-deoxy-1-C-<(phenylthio)bis(methoxycarbonyl)methyl>-2,3,5-tri-O-benzyl-D-ribofuranose

β-1-deoxy-1-C-(phenylthio)-2,3,5-tri-O-benzyl-D-ribofuranose

α-1-deoxy-1-C-(phenylthio)-2,3,5-tri-O-benzyl-D-ribofuranose

Downstream raw materials:

α-1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose

β-1-deoxy-1-C--2,3,5-tri-O-benzyl-D-ribofuranose

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