tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

Base Information

Chemical Name:tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate
CAS No.:1237739-36-4
Molecular Formula:C₁₂H₃₆P₄Rh*C₂₄BF₂₀
Molecular Weight:1086.26
Hs Code.:

Synonyms:tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

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Chemical Property of tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

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Technology Process of tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

There total 1 articles about tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 70525-09-6,92670-96-7
[rhodium(I)(trimethylphosphine)4](chloride)

: 148354-27-2
triethylsilylium tetrakis(pentafluorophenyl), toluene adduct

: 1237739-36-4
tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

Guidance literature:: In toluene; stoich., soln. of Et3SiB(C6F5)4 in toluene added to suspn. of Rh complexin toluene at 25°C, stirred for 12 h; cooled to -10°C, crystd., collected, dried (vac.), elem. anal.;
DOI:10.1039/c0cc00892c

Reference yield: 77.0%

: 1237739-36-4
tetrakis(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

: 594-09-2
trimethylphosphane

: 1237739-38-6
penta(triphenylphosphine)Rh(I)(tetrakis(pentafluorophenyl)borate

Guidance literature:: In neat (no solvent); (vac.), Rh complex dissolved in PMe3 at 80°C for 1 h; cooled to room temp., pptd., dried (vac.), elem. anal.;
DOI:10.1039/c0cc00892c