9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

Base Information

Chemical Name:9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide
CAS No.:291546-11-7
Molecular Formula:C₄₄H₄₄N₂O₆
Molecular Weight:696.843
Hs Code.:

Synonyms:9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

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Technology Process of 9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

There total 2 articles about 9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 291546-10-6
9-Amino-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

: 291546-11-7
9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 45 ℃; for 6h;
DOI:10.1002/1521-3765(20001103)6:21<3984::AID-CHEM3984>3.0.CO;2-F

Reference yield:

: 291546-11-7
9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

Guidance literature:

Reference yield:

: 291546-11-7
9-(N,N-Di-tert-butoxycarbonylamino)-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboxamide

: 9-(Di-sec-butoxycarbonyl)amino-N-(2,6-diisopropylphenyl)perylene-3,4-dicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: 200 °C

2: 77 percent / 4-dimethylaminopyridine; Et₃N / tetrahydrofuran / 6 h / 45 °C

With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1002/1521-3765(20001103)6:21<3984::AID-CHEM3984>3.0.CO;2-F