[(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate

Base Information

• Chemical Name: [(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate
• CAS No.: 1620661-08-6
• Molecular Formula: CF₃O₃S*C₂₄H₄₄N₂PSe
• Molecular Weight: 619.631

Synonyms:[(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate

Chemical Property of [(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate

Chemical Property:

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Technology Process of [(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate

There total 1 articles about [(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

C17H30NPSe (1620661-04-2) + 1,1,5,5-Tetraisopropyl-1,5-diazonia-3-oxapent-1,4-dienyl bis(trifluoromethanesulfonate) → [(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate (1620661-08-6)

Guidance literature:

at 0 - 20 ℃; for 3h;

DOI:10.1002/ejic.201402166

Reference yield: 99.0%

[(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate (1620661-08-6) → [(di-tert-butylphosphanyl)-2,4,6-trimethylphenylamino]methylenediisopropylammonium trifluoromethanesulfonate (1620661-18-8)

Guidance literature:

With Hexamethylphosphorous triamide; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1002/ejic.201402166

Reference yield: 88.0%

[(di-tert-butylphosphanylselenoyl)-2,4,6-trimethylphenylmethylene]-diisopropylaminoammonium trifluoromethanesulfonate (1620661-08-6) → N'-(2-{[di-tert-butyl(selanylidene)-λ5-phosphanyl]methyl}-4,6-dimethylphenyl)-N,N-bis(propan-2-yl)methanimidamide

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -90 - 20 ℃; for 1h;

DOI:10.1002/ejic.201402166

upstream raw materials:

C₁₇H₃₀NPSe

Downstream raw materials:

[(di-tert-butylphosphanyl)-2,4,6-trimethylphenylamino]methylenediisopropylammonium trifluoromethanesulfonate

C₂₄H₄₃N₂P

1,1-di-tert-butyl-N,N-diisopropyl-N'-(2,4,6-trimethylphenyl)phosphanylcarboximidamide

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