Technology Process of C31H44N6O7
There total 5 articles about C31H44N6O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrazine;
In
methanol;
Ambient temperature;
DOI:10.1021/ja972670j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) ethyl chloroformate, N-methylmorpholine / 1.) EtOAc, 0 deg C, 3 h, 2.) EtOAc, ether, room temp., overnight
2: Et3N, silver benzoate / Ambient temperature
3: 100 percent / aq. NaOH / dioxane / 1 h / Ambient temperature
4: 74 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride, 4-methylmorpholine / CH2Cl2 / Ambient temperature
5: 52 percent / N2H4 / methanol / Ambient temperature
With
4-methyl-morpholine; sodium hydroxide; silver benzoate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; chloroformic acid ethyl ester; triethylamine; hydrazine;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ja972670j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N, silver benzoate / Ambient temperature
2: 100 percent / aq. NaOH / dioxane / 1 h / Ambient temperature
3: 74 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride, 4-methylmorpholine / CH2Cl2 / Ambient temperature
4: 52 percent / N2H4 / methanol / Ambient temperature
With
4-methyl-morpholine; sodium hydroxide; silver benzoate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; hydrazine;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ja972670j