trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

Base Information

Chemical Name:trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol
CAS No.:97151-05-8
Molecular Formula:C₂₇H₃₁NO₂
Molecular Weight:401.549
Hs Code.:

Synonyms:trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

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Chemical Property of trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

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Technology Process of trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

There total 8 articles about trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 503-30-0
trimethylene oxide

: 19118-19-5
trans-(E)-1-bromo-2-<4-<2-(dimethylamino)ethoxy>phenyl>-1,2-diphenylethene

: 97151-11-6
trans-(Z)-1-<4-<2-(dimethylamino)ethoxy>phenyl>-1,2-diphenylethylene

: 97151-05-8
trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

: 97151-06-9
cis-(E)-1-<4-<2-(dimethylamino)ethoxy>phenyl>-1,2-diphenyl-1-penten-5-ol

Guidance literature:: With n-butyllithium; In hexane; for 1h; Ambient temperature;
DOI:10.1021/jm00148a020

Reference yield:

: C₂₇H₃₀BrNO₂

: 97151-05-8
trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2016.04.076

Reference yield:

: (E)-methyl 5-(4-bromophenyl)-5-(4-hydroxyphenyl)-4-phenylpent-4-enoate

: 97151-05-8
trans-(Z)-1-{4-[2-(dimethylamino)ethoxy]phenyl}-1,2-diphenyl-1-penten-5-ol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 60 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/j.ejmech.2016.04.076