1-(1-Hydroxy-allyl)-cyclohexanol

Base Information

Chemical Name:1-(1-Hydroxy-allyl)-cyclohexanol
CAS No.:59906-45-5
Molecular Formula:C₉H₁₆O₂
Molecular Weight:156.225
Hs Code.:

Synonyms:1-(1-Hydroxy-allyl)-cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1-Hydroxy-allyl)-cyclohexanol

Chemical Property:

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Technology Process of 1-(1-Hydroxy-allyl)-cyclohexanol

There total 7 articles about 1-(1-Hydroxy-allyl)-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2-tosylimino-4-vinyl-1,3-dioxaspiro[4.5]decane

: 59906-45-5
1-(1-Hydroxy-allyl)-cyclohexanol

Guidance literature:: With water; sodium hydroxide; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201200378

Reference yield:

: 59906-46-6
1-(1-Trimethylsilanyloxy-allyl)-cyclohexanol

: 59906-45-5
1-(1-Hydroxy-allyl)-cyclohexanol

Guidance literature:: With acetic acid; In tetrahydrofuran;
DOI:10.1021/jo00884a031

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 59906-45-5
1-(1-Hydroxy-allyl)-cyclohexanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 0 °C / Molecular sieve; Inert atmosphere

3.2: 0 °C / Molecular sieve; Inert atmosphere

4.1: tetrahydrofuran / 0 - 20 °C / Molecular sieve; Inert atmosphere

5.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: sodium hydroxide; water / methanol / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/ejoc.201200378