1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

Base Information

Chemical Name:1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan
CAS No.:1185773-84-5
Molecular Formula:C₄₇H₃₆O₁₁
Molecular Weight:776.796
Hs Code.:

Synonyms:1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

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Chemical Property of 1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

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Technology Process of 1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

There total 1 articles about 1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1185773-79-8
1,5,9-tribromo-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1185773-84-5
1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,2-dimethoxyethane; water; at 65 - 70 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo9013047

Reference yield: 100.0%

: 1185773-84-5
1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

: 1185773-85-6
1,5,9-tri-carboxylbonylphenyl-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan

Guidance literature:: 1,5,9-tri-(4-methoxycarbonylphenyl)-12c-(2-(methoxymethoxy)ethyl)-4,8,12-trioxatricornan; With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 0 - 20 ℃; for 24h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃; pH=4;
DOI:10.1021/jo9013047