N-propynyl sulforhodamine B

Base Information

Chemical Name:N-propynyl sulforhodamine B
CAS No.:1092380-67-0
Molecular Formula:C₃₀H₃₃N₃O₆S₂
Molecular Weight:595.741
Hs Code.:

Synonyms:N-propynyl sulforhodamine B

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Chemical Property of N-propynyl sulforhodamine B

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Technology Process of N-propynyl sulforhodamine B

There total 1 articles about N-propynyl sulforhodamine B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 15430-52-1
prop-2-yn-1-amine hydrochloride

: 62796-29-6
rhodamine B sulfonyl chloride

: 1092380-67-0
N-propynyl sulforhodamine B

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3ob42332h

Reference yield: 43.0%

: 1541175-37-4
(2S)-2-((2S,4R)-4-azido-1-(phenylsulfonyl)pyrrolidine-2-carboxamido)-3-(4-((pyrrolidine-1-carbonyl)oxy)phenyl)propanoic acid

: 1092380-67-0
N-propynyl sulforhodamine B

: 1541175-39-6
R-BC₁₅₄

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 60 ℃; for 2h;
DOI:10.1039/c3ob42332h

Reference yield:

: 1541175-37-4
(2S)-2-((2S,4R)-4-azido-1-(phenylsulfonyl)pyrrolidine-2-carboxamido)-3-(4-((pyrrolidine-1-carbonyl)oxy)phenyl)propanoic acid

: 1092380-67-0
N-propynyl sulforhodamine B

: C₅₅H₆₀N₉O₁₃S₃^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: sodium L-ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 60 °C

2: sodium hydroxide

With copper(II) sulfate; sodium L-ascorbate; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42332h