N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

Base Information

Chemical Name:N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride
CAS No.:1567842-43-6
Molecular Formula:C₂₃H₂₉ClN₂O*ClH
Molecular Weight:421.41
Hs Code.:

Synonyms:N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

Chemical Property:

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Technology Process of N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

There total 5 articles about N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1570522-61-0
N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide

: 1567842-43-6
N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether;
DOI:10.1016/j.bmcl.2014.01.032

Reference yield:

: 1567842-52-7
(E)-N-ethylidene-1-(piperidin-4-yl)methanamine

: 1567842-43-6
N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 12 h / Reflux

2: sodium tetrahydroborate / methanol / 20 °C

3: triethylamine / tetrahydrofuran / 24 h / 0 °C

4: hydrogenchloride / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; diethyl ether; acetone;
DOI:10.1016/j.bmcl.2014.01.032

Reference yield:

: 1272306-01-0
N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)ethanamine

: 1567842-43-6
N-((1-(4-chlorobenzyl)piperidin-4-yl)methyl)-N-ethyl-4-methylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 24 h / 0 °C

2: hydrogenchloride / diethyl ether

With hydrogenchloride; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmcl.2014.01.032