2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

Base Information

Chemical Name:2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid
CAS No.:768340-27-8
Molecular Formula:C₂₄H₂₃NO₅S
Molecular Weight:437.516
Hs Code.:

2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

Synonyms:2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

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Chemical Property of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

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Technology Process of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

There total 4 articles about 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 152953-56-5
Fmoc-Phe-ψ[CH2-SH]

: 768340-27-8
2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

Guidance literature:: With formic acid; dihydrogen peroxide; In water; at 0 - 20 ℃;
DOI:10.1055/s-0029-1219584

Reference yield:

: 152953-55-4
thioacetic acid S-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propyl] ester

: 768340-27-8
2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

Guidance literature:: With dihydrogen peroxide; acetic acid; at 20 ℃;
DOI:10.1055/s-2000-7615

Reference yield:

: 129397-83-7
(9-fluorenylmethoxycarbonyl)-L-phenylalaninol

: 768340-27-8
2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-phenyl-propane-1-sulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 °C

2: caesium carbonate / N,N-dimethyl-formamide / 20 °C

3: water; dihydrogen peroxide; acetic acid / 20 °C

With water; dihydrogen peroxide; caesium carbonate; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.02.014