4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

Base Information

Chemical Name:4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate
CAS No.:73127-59-0
Molecular Formula:C₂₈H₃₇IO₆S
Molecular Weight:628.569
Hs Code.:

Synonyms:4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

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Chemical Property of 4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

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Technology Process of 4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

There total 29 articles about 4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 111649-56-0
4-<2-(4-methanesulfonyloxy butyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

: 73127-59-0
4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

Guidance literature:: With sodium hydrogencarbonate; sodium iodide; In acetone; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90012-2

Reference yield:

: 74726-78-6
1-iodo-2-phenylthiomethyl-4,6-dimethoxy-benzene

: 73127-59-0
4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

Guidance literature:: With potassium carbonate; palladium dichloride; In benzene; at 120 ℃; for 16h; under 9120 Torr;
DOI:10.1246/cl.1980.369

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 73127-59-0
4-<2-(4-iodobutyl)-1,3-dioxalan-2-yl>-1-methylbutyl-2,4-dimethoxy-6-<(phenylthio) methyl> benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / CCl₄ / 6 h / Heating; Irradiation

2: 52 percent / lithium aluminium hydride / diethyl ether / 0 °C

3: 1.) n-BuLi, 2.) iodine / 1.) THF, -78 deg C, 2.) -40 deg C

4: SOCl₂

5: sodium ethoxide

6: 70 percent Chromat_. / K₂CO₃ / PdCl₂ / benzene / 16 h / 120 °C / 9120 Torr

With lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; bromine; iodine; sodium ethanolate; potassium carbonate; palladium dichloride; In tetrachloromethane; diethyl ether; benzene;
DOI:10.1246/cl.1980.369