(R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

Base Information

Chemical Name:(R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid
CAS No.:1198185-98-6
Molecular Formula:C₁₇H₁₉N₃O₄
Molecular Weight:329.356
Hs Code.:

Synonyms:(R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

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Chemical Property of (R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

Chemical Property:

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Technology Process of (R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

There total 1 articles about (R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198185-95-3
(R)-3-(1-allyl-1H-imidazol-4-yl)-2-aminopropionic acid

: 501-53-1,94274-21-2
benzyl chloroformate

: 1198185-98-6
(R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

Guidance literature:: (R)-3-(1-allyl-1H-imidazol-4-yl)-2-aminopropionic acid; benzyl chloroformate; With sodium hydroxide; at 0 ℃; for 2h;

With hydrogenchloride; In water; pH=3 - 4;

Reference yield:

: 1198185-98-6
(R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

: 500708-37-2
(S)-1-(allyloxy)-3-methylbutan-2-amine

: 1198186-00-3
benzyl [(R)-2-(1-allyl-1H-imidazol-4-yl)-1-((S)-1-allyloxymethyl-2-methylpropylcarbamoyl)ethyl]carbamate

Guidance literature:: (R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

(S)-1-(allyloxy)-3-methylbutan-2-amine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

: 1198185-98-6
(R)-3-(1-Allyl-1H-imidazol-4-yl)-2-benzyloxycarbonylaminopropionic acid

: 1198186-02-5
benzyl ((8S,11R)-8-isopropyl-10-oxo-6-oxa-1,9,14-triazabicyclo[11.2.1]hexadeca-3,13⁽¹⁶⁾,14-trien-11-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 2 h / 20 °C

1.2: 24 h / 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; N,N-dimethyl-formamide;