butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate

Base Information

Chemical Name:butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate
CAS No.:912838-01-8
Molecular Formula:C₂₂H₃₀N₄O₄
Molecular Weight:414.505
Hs Code.:

Synonyms:butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate

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Chemical Property of butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate

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Technology Process of butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate

There total 1 articles about butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 30414-57-4
methyl 3-oxohept-6-enoate

: 71026-66-9
N-(tert-butoxycarbonyl)-1,4-phenylenediamine

: 79791-38-1
4-dodecylbenzenesulphonyl azide

: 912838-01-8
butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: methyl 3-oxohept-6-enoate; N-(tert-butoxycarbonyl)-1,4-phenylenediamine; butan-1-ol; With sulfuric acid; for 6h; Heating / reflux;

4-dodecylbenzenesulphonyl azide; With triethylamine; In acetonitrile; at 20 ℃; for 6h; Heating / reflux;

With sodium nitrite; In water; acetonitrile; at 20 ℃;

Reference yield: 70.0%

: 912838-01-8
butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate

: C₁₈H₂₂N₄O₄

Guidance literature:: butyl 5-(3-buten-1-yl)-1-{4-[(tert-butoxycarbonyl)amino]phenyl}-1H-1,2,3-triazole-4-carboxylate; With sodium hydroxide; water; In tetrahydrofuran; methanol; at 20 ℃; for 4h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;