ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

Base Information

Chemical Name:ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate
CAS No.:123753-66-2
Molecular Formula:C₁₇H₁₈N₆O₃
Molecular Weight:354.368
Hs Code.:

Synonyms:ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

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Chemical Property of ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

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Technology Process of ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

There total 6 articles about ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 123753-65-1
ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>-2(3H)-thioxoimidazo<4,5-c>pyridin-6-yl>carbamate

: 123753-66-2
ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: With nickel; In ethanol; at 2.5 ℃; Heating;
DOI:10.1021/jm00164a030

Reference yield:

: 109182-40-3
ethyl (6-amino-4-hydrazino-5-nitropyridin-2-yl)carbamate

: 123753-66-2
ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Raney nickel / ethanol; H₂O / 1 h / 23 °C / 760 Torr

2: Et₃N / N,N-dimethyl-acetamide / 40 h / Ambient temperature

3: 29 percent / conc. H₂SO₄ / N,N-dimethyl-acetamide / 2.5 h / 93 °C

4: 14 percent / Raney nickel / ethanol / 2.5 °C / Heating

With sulfuric acid; hydrogen; nickel; triethylamine; nickel; In ethanol; N,N-dimethyl acetamide; water;
DOI:10.1021/jm00164a030

Reference yield:

: 123753-53-7
ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

: 123753-66-2
ethyl N-<4-amino-1-<(4-methoxybenzylidene)amino>imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / H₂ / Raney nickel / N,N-dimethyl-acetamide / 1.83 h / 760 Torr / Ambient temperature

2: 12 percent / Et₃N / N,N-dimethyl-acetamide / 23 h / Ambient temperature

3: 29 percent / conc. H₂SO₄ / N,N-dimethyl-acetamide / 2.5 h / 93 °C

4: 14 percent / Raney nickel / ethanol / 2.5 °C / Heating

With sulfuric acid; hydrogen; nickel; triethylamine; nickel; In ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jm00164a030