2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Base Information

Chemical Name:2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester
CAS No.:118317-29-6
Molecular Formula:C₂₆H₂₃NO₄
Molecular Weight:413.473
Hs Code.:

Synonyms:2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Suppliers and Price of 2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

There total 6 articles about 2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 118317-24-1
2-Cyclopropyl-acrylic acid 1-formyl-naphthalen-2-yl ester

: 24461-61-8,26682-99-5,37760-98-8,6591-61-3
phenylglycine methyl ester

: 118317-29-6
2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Guidance literature:: With sodium sulfate; In dichloromethane; reflux 1 h, r.t. 10 h;
DOI:10.1016/S0040-4020(01)85931-7

Reference yield:

: 6395-79-5
methyl 2-cyclopropyl-2-oxoacetate

: 118317-29-6
2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-butyl lithium / 1.) 4 h, r.t., ether, hexan; 2.) ether, r.t., 15 h

2: 69 percent / sodium hydroxide / H₂O; ethanol / 3 h / Heating

3: 1.) dicyclohexylcarbodiimide, p-toluenesulphonic acid; 2.) g. acetic acid / 1.) pyridine, 24 h; 2.) 2 h, r.t., 0 degC, overnight

4: 95 percent / sodium sulphate / CH₂Cl₂ / reflux 1 h, r.t. 10 h

With sodium hydroxide; n-butyllithium; toluene-4-sulfonic acid; acetic acid; sodium sulfate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1016/S0040-4020(01)85931-7

Reference yield:

: 13266-09-6
methylenecyclopropylacetic acid

: 118317-29-6
2-Cyclopropyl-acrylic acid 1-{[(E)-methoxycarbonyl-phenyl-methylimino]-methyl}-naphthalen-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dicyclohexylcarbodiimide, p-toluenesulphonic acid; 2.) g. acetic acid / 1.) pyridine, 24 h; 2.) 2 h, r.t., 0 degC, overnight

2: 95 percent / sodium sulphate / CH₂Cl₂ / reflux 1 h, r.t. 10 h

With toluene-4-sulfonic acid; acetic acid; sodium sulfate; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0040-4020(01)85931-7