anti-α-(p-Tolylthio)acetophenone oxime

Base Information

• Chemical Name: anti-α-(p-Tolylthio)acetophenone oxime
• CAS No.: 50314-81-3
• Molecular Formula: C₁₅H₁₅NOS
• Molecular Weight: 257.356
• Mol file: 50314-81-3.mol

Synonyms:anti-α-(p-Tolylthio)acetophenone oxime

Chemical Property of anti-α-(p-Tolylthio)acetophenone oxime

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of anti-α-(p-Tolylthio)acetophenone oxime

There total 2 articles about anti-α-(p-Tolylthio)acetophenone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

para-thiocresol (106-45-6) + N-(1-phenylvinyl)-O-(trimethylsilyl)-N-((trimethylsilyl)oxy)hydroxylamine (344899-62-3) → anti-α-(p-Tolylthio)acetophenone oxime (50314-81-3)

Guidance literature:

In toluene; at 20 ℃; for 24h;

DOI:10.1055/s-0036-1591973

Reference yield:

→ anti-α-(p-Tolylthio)acetophenone oxime (50314-81-3)

Guidance literature:

Ketal 3b, HCl;

DOI:10.1021/jo00919a039

upstream raw materials:

para-thiocresol

N-(1-phenylvinyl)-O-(trimethylsilyl)-N-((trimethylsilyl)oxy)hydroxylamine