N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

Base Information

Chemical Name:N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide
CAS No.:315234-84-5
Molecular Formula:C₃₈H₅₄N₆O₄
Molecular Weight:658.885
Hs Code.:

Synonyms:N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

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Chemical Property of N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

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Technology Process of N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

There total 4 articles about N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 112-13-0
n-decanoyl chloride

: 252903-90-5
N,N'-bis(6-aminopyridin-2-yl)-5-decyloxyisophthalimide

: 5-decyloxy-N,N'-bis[6-(decanoylamino)pyridin-2-yl]-isophthalimide

: 315234-84-5
N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/1521-3765(20000602)6:11<1938::AID-CHEM1938>3.0.CO;2-Y

Reference yield:

: 112-29-8
1-bromo dodecane

: 315234-84-5
N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 20 °C

2: BuLi / tetrahydrofuran / -78 °C

3: 32 percent / NEt₃ / tetrahydrofuran / 1 h / 0 °C

With n-butyllithium; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Etherification / 2: Acylation / 3: Acylation;
DOI:10.1002/1521-3765(20000602)6:11<1938::AID-CHEM1938>3.0.CO;2-Y

Reference yield:

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 315234-84-5
N-(6-Aminopyridin-2-yl)-N'-(6-decanoylaminopyridin-2-yl)-5-decyloxyisophthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 20 °C

2: BuLi / tetrahydrofuran / -78 °C

3: 32 percent / NEt₃ / tetrahydrofuran / 1 h / 0 °C

With n-butyllithium; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Etherification / 2: Acylation / 3: Acylation;
DOI:10.1002/1521-3765(20000602)6:11<1938::AID-CHEM1938>3.0.CO;2-Y