4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

Base Information

Chemical Name:4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide
CAS No.:1422064-44-5
Molecular Formula:C₃₂H₃₀ClN₅O₄
Molecular Weight:584.074
Hs Code.:

Synonyms:4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

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Chemical Property of 4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

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Technology Process of 4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

There total 5 articles about 4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.5%

: 2233-18-3
4-hydroxy-3,5-dimethylbenzaldehyde

: 1422064-41-2
4-chloro-2-[2-(hydrazinecarbonyl)phenylamino]benzohydrazide

: 1422064-44-5
4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

Guidance literature:: With acetic acid; In ethanol; Reflux;
DOI:10.1248/cpb.c12-00516

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 1422064-44-5
4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: copper(II) oxide

2: thionyl chloride / 4 h / Reflux

3: hydrazine hydrate / butan-1-ol / 25 h / Reflux

4: acetic acid / ethanol / Reflux

With thionyl chloride; hydrazine hydrate; acetic acid; copper(II) oxide; In ethanol; butan-1-ol; 1: |Ullmann Condensation;
DOI:10.1248/cpb.c12-00516

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 1422064-44-5
4-chloro-N'-(4-hydroxy-3,5-dimethylbenzylidene)-2-{2-[2(4-hydroxy-3,5-dimethylbenzylidene)hydrazinecarbonyl]phenylamino}benzohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: copper(II) oxide

2: thionyl chloride / 4 h / Reflux

3: hydrazine hydrate / butan-1-ol / 25 h / Reflux

4: acetic acid / ethanol / Reflux

With thionyl chloride; hydrazine hydrate; acetic acid; copper(II) oxide; In ethanol; butan-1-ol; 1: |Ullmann Condensation;
DOI:10.1248/cpb.c12-00516